relation: http://publicatio.bibl.u-szeged.hu/30630/ title: Obtaining and physical-chemical characterization of inclusion complex of a sulphonamidic diuretic with methylated beta-cyclodextrine [Objinerea §i caracterizarea fizico-chimicä a compu§ilor de incluziune ai unui diuretic sulfonamidic cu ß-ciclodextrinä metilatä] creator: Soica C. creator: Gyéresi Árpád creator: Aigner Zoltán creator: Kata Mihály creator: Dehelean C. subject: 01.04. Kémiai tudományok subject: 03.01. Általános orvostudomány description: Furosemide is a practically insoluble in water sulphonamidic diuretic, used for the treatment of edema and hypertension. Randomly-methylated-beta-cyclodextrin(RAMEB) was used as a host molecule to improve its solubility in water, via inclusion complex formation. Different molar ratios (1: 1, 1:2) and various preparation methods (physical mixing, kneading, ultrasonication) were used in order to obtain the inclusion complexes. Phase solubility diagram of furosemide and RAMEB was constructed and a diagram of A(L) type was obtained, with a stability constant of 130 M-1. The inclusion complexes were analysed by in vitro dissolution tests, differential scanning calorimetry and X-ray diffraction. As water solubility increased, the partition coefficients of the products decreased. date: 2006 type: Folyóiratcikk type: PeerReviewed format: text identifier: http://publicatio.bibl.u-szeged.hu/30630/1/aok_klny_318_06.pdf identifier: Soica C.; Gyéresi Árpád; Aigner Zoltán; Kata Mihály; Dehelean C.: Obtaining and physical-chemical characterization of inclusion complex of a sulphonamidic diuretic with methylated beta-cyclodextrine [Objinerea §i caracterizarea fizico-chimicä a compu§ilor de incluziune ai unui diuretic sulfonamidic cu ß-ciclodextrinä metilatä]. REVISTA DE CHIMIE, 57 (4). pp. 392-397. ISSN 0034-7752 (2006) relation: 1883473 language: rum